高强混凝土内养护效果的微观量化表征与分析
作者:
作者单位:

1.华北水利水电大学 水利学院,河南 郑州 450046;2.河南水谷研究院,河南 郑州 450046;3.华北水利水电大学 河南省水环境模拟与治理重点实验室,河南 郑州 450002;4.河南省 信阳水文水资源勘测局,河南 信阳 464000

作者简介:

郭利霞(1982—),女,河南开封人,华北水利水电大学副教授,硕士生导师,博士.E-mail:guolx@126.com

通讯作者:

钟 凌(1982—),男,湖南邵阳人,华北水利水电大学讲师,硕士生导师,博士.E-mail: 250514782@qq.com

中图分类号:

TU528.31

基金项目:

国家自然科学基金资助项目(52109154);河南省自然科学基金资助项目(202300410270)


Microscopic Quantitative Characterization and Analysis of Internal Curing Effect of High Strength Concrete
Author:
Affiliation:

1.School of Water Conservancy, North China University of Water Resources and Electric Power, Zhengzhou 450046, China;2.Henan Water Valley Research Institute, Zhengzhou 450046, China;3.Henan Key Laboratory of Water Environment Simulation and Treatment, North China University of Water Resources and Electric Power, Zhengzhou 450002, China;4.Xinyang Hydrological and Water Resources Survey Bureau of Henan Province, Xinyang 464000, China

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    摘要:

    采用高吸水性树脂(SAP)作为混凝土内养护材料,通过纳米压痕试验,研究了养护龄期和SAP掺量对内养护混凝土孔洞界面微观力学的影响,借助扫描电镜与能谱分析(SEM-EDS)表征混凝土的内部物相及化学组成.结果表明:随着养护龄期的增加,SAP释水界面的弹性模量和硬度提高;掺入SAP后,混凝土中的水化产物分布更加均匀;随着养护龄期的增加,水化产物含量逐渐增大,界面更加致密;SEM-EDS测试结果与力学性能相吻合,说明SAP对高强混凝土具有积极影响.

    Abstract:

    Super absorbent polymer (SAP) was used as the internal curing material for concrete. Through the nanoindentation test, the effects of curing age and SAP content on the micromechanics of the cavity interface of the internally cured concrete were studied, and the internal phase and chemical composition of the concrete were characterized by scanning electron microscope and energy dispersive spectroscopy (SEM-EDS). The results show that the elastic modulus and hardness of the SAP water release interface increase with the increase of curing age. After adding SAP, the distribution of hydration products in concrete becomes more uniform. As the curing age increases, the content of hydration products gradually increases, and the interface becomes denser. The SEM-EDS test results are consistent with the test of mechanical properties, indicating that SAP has a positive impact on high-strength concrete.

    表 3 混凝土的配合比Table 3 Mix proportions of concretes
    表 1 粗骨料的物理性质Table 1 Physical properties of coarse aggregates
    图1 纳米压痕测试原理示意图和荷载-位移曲线Fig.1 Principle sketch map and load-displacement curve of nano indentation test
    图2 试样压痕试验区域照片Fig.2 Photographs of indentation test area of samples
    图3 内养护混凝土的弹性模量与硬度分布云图Fig.3 Elastic modulus and hardness distribution cloud maps of internal curing concrete
    图4 混凝土中SAP释水过程示意图Fig.4 Schematic of water release process of SAP in concrete
    图5 不同养护龄期下试样HSC10的EDS图谱Fig.5 EDS spectra of sample HSC10 at different curing ages
    图6 试样HSC和HSC10的弹性模量及硬度分布云图Fig.6 Elastic modulus and hardness distribution cloud maps of sample HSC and HSC10
    图7 试样HSC和HSC10的SEM照片(7 d养护龄期)Fig.7 SEM images of sample HSC and HSC10(curing age is 7 d)
    图8 试样HSC与HSC10的EDS图谱Fig.8 EDS spectra of sample HSC and HSC10
    表 2 水泥及各掺合料的主要化学组成Table 2 Main chemical compositions of cement and each admixture
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引用本文

郭利霞,武铮,钟凌,张芳芳,罗云.高强混凝土内养护效果的微观量化表征与分析[J].建筑材料学报,2023,26(7):697-704

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  • 收稿日期:2022-08-09
  • 最后修改日期:2022-11-05
  • 在线发布日期: 2023-09-15
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